BF₂-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine

Base Information

• Chemical Name: BF₂-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine
• CAS No.: 1021175-75-6
• Molecular Formula: C₃₆H₃₂BF₂N₅
• Molecular Weight: 583.491

Synonyms:BF₂-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine

Chemical Property of BF₂-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine

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Technology Process of BF₂-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine

There total 7 articles about BF₂-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine → BF2-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine (1021175-75-6)

Guidance literature:

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/b713020a

Reference yield: 53.0%

[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine (873975-73-6) + boron trifluoride diethyl etherate (109-63-7) → BF2-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine (1021175-75-6)

Guidance literature:

With diisopropylethylamine; In dichloromethane; under N2; ligand dissolved in dry CH2Cl2; treated with i-Pr2NEt and BF3(OEt2); stirred at room temp. for 24 h; washed with H2O; org. layer dried (Na2SO4); evapd. to dryness; purified by column chromy. (silica gel, CH2Cl2-hexane 3:1); elem. anal.;

DOI:10.1039/b713020a

Reference yield:

[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine (873975-73-6) → BF2-chelated-[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine (1021175-75-6)

Guidance literature:

[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.25h; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.2174/157017811796064377

upstream raw materials:

[3-(4-dimethylaminophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-dimethylaminophenyl)-5-phenylpyrrol-2-ylidene]amine

boron trifluoride diethyl etherate

3-[4-(dimethylamino)phenyl]-4-nitro-1-phenylbutan-1-one

acetophenone

Downstream raw materials:

C₃₈H₃₈BN₅O₂

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