2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate
CAS No.:952685-73-3
Molecular Formula:C₁₉H₄₂N₂O₃Si₂
Molecular Weight:402.725
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Suppliers and Price of 2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

There total 7 articles about 2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-77-4
chloro-trimethyl-silane

: 952685-57-3
2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-hydroxybutylcarbamate

: 952685-73-3
2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.666667h;

Reference yield:

: 952685-48-2
tert-butyl (2S,3R)-4-chloro-1-cyclohexyl-3-hydroxybutan-2-ylcarbamate

: 952685-73-3
2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / ethanol / 1 h

2: ammonium hydroxide / methanol; water / 20 °C

3: potassium carbonate / water; acetone / 2 h / 20 °C

4: toluene-4-sulfonic acid / diethyl ether; ethanol / 20 - 65 °C

5: triethylamine / dichloromethane / 0.67 h / 0 - 20 °C

With sodium hydroxide; potassium carbonate; toluene-4-sulfonic acid; ammonium hydroxide; triethylamine; In methanol; diethyl ether; ethanol; dichloromethane; water; acetone;

Reference yield:

: 952685-56-2
2-(trimethylsilyl)ethyl (2S,3S)-3-tert-butoxycarbonylamino-4-cyclohexyl-2-hydroxybutylcarbamate

: 952685-73-3
2-(trimethylsilyl)ethyl (2S,3S)-3-amino-4-cyclohexyl-2-(trimethylsilyloxy)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / diethyl ether; ethanol / 20 - 65 °C

2: triethylamine / dichloromethane / 0.67 h / 0 - 20 °C

With toluene-4-sulfonic acid; triethylamine; In diethyl ether; ethanol; dichloromethane;