Technology Process of C27H32O4Si
There total 9 articles about C27H32O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
SiO2-supported NaIO4;
In
dichloromethane;
at 0 - 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1016/j.tet.2011.10.058
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere
2.1: tetrahydrofuran / 6 h / -20 - 20 °C / Inert atmosphere
3.1: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
4.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 8 h / 20 °C / Inert atmosphere
4.2: 1 h / 20 °C / Inert atmosphere
5.1: SiO2-supported NaIO4 / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
With
1H-imidazole; osmium(VIII) oxide; SiO2-supported NaIO4; water; potassium carbonate; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; methanol; dichloromethane; acetone; tert-butyl alcohol;
4.1: Upjohn dihydroxylation;
DOI:10.1016/j.tet.2011.10.058
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
2.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 8 h / 20 °C / Inert atmosphere
2.2: 1 h / 20 °C / Inert atmosphere
3.1: SiO2-supported NaIO4 / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
With
1H-imidazole; osmium(VIII) oxide; SiO2-supported NaIO4; water; 4-methylmorpholine N-oxide;
In
dichloromethane; acetone; tert-butyl alcohol;
2.1: Upjohn dihydroxylation;
DOI:10.1016/j.tet.2011.10.058
