(S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

Base Information

Chemical Name:(S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate
CAS No.:1151539-51-3
Molecular Formula:C₁₆H₂₃N₃O₅
Molecular Weight:337.376
Hs Code.:

Synonyms:(S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

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Technology Process of (S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

There total 3 articles about (S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4070-48-8
L-Valine methyl ester

: 50622-95-2
benzyl (2-azido-2-oxoethyl)carbamate

: 1151539-51-3
(S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

Guidance literature:: In toluene; at 45 ℃; Sonication;
DOI:10.1055/s-0033-1340864

Reference yield: 83.0%

: 4070-48-8
L-Valine methyl ester

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1151539-51-3
(S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

Guidance literature:: N-(Benzyloxycarbonyl)glycine; With trimethylsilylazide; triethylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at 0 ℃; Sonication;

L-Valine methyl ester; In dichloromethane; Sonication;
DOI:10.1055/s-0028-1087538

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1151539-51-3
(S)-methyl 9-isopropyl-3,7-dioxo-1-phenyl-2-oxa-4,6,8-triazadecan-10-oate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; 3,3-dichloro-1,2-diphenylcyclopropene; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / -15 °C

2: toluene / 45 °C / Sonication

With oxalyl dichloride; 3,3-dichloro-1,2-diphenylcyclopropene; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; 2: |Curtius Rearrangement;
DOI:10.1055/s-0033-1340864