N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

Base Information

Chemical Name:N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine
CAS No.:1007308-60-2
Molecular Formula:C₁₇H₁₅ClN₄O₄
Molecular Weight:374.783
Hs Code.:

N<sub>4</sub>-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

Synonyms:N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

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Chemical Property of N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

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Technology Process of N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

There total 3 articles about N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.5%

: 1007308-59-9
C₁₆H₁₂Cl₂N₄O₃

: 124-41-4
sodium methylate

: 1007308-60-2
N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

Guidance literature:: In methanol; for 16h; Heating / reflux;

Reference yield:

: 53449-14-2
7-chloro-6-nitro-4(3H)-quinazolinone

: 1007308-60-2
N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / N,N-dimethyl-formamide / 17 h / 20 °C / Heating / reflux

2: triethylamine / N,N-dimethyl-formamide / isopropyl alcohol / 17 h / 20 °C

3: methanol / 16 h / Heating / reflux

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In methanol; isopropyl alcohol;

Reference yield:

: 162012-71-7
4,7-dichloro-6-nitro-quinazoline

: 1007308-60-2
N₄-(3-chloro-4-methoxy-benzyl)-(7-methoxy-6-nitro-quinazolin-4-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / isopropyl alcohol / 17 h / 20 °C

2: methanol / 16 h / Heating / reflux

With triethylamine; N,N-dimethyl-formamide; In methanol; isopropyl alcohol;