(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

Base Information

Chemical Name:(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine
CAS No.:1442445-64-8
Molecular Formula:C₁₅H₁₃BrClF₃N₂
Molecular Weight:393.634
Hs Code.:

Synonyms:(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

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Technology Process of (R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

There total 5 articles about (R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1442445-41-1
(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-2-nitroaniline

: 64-19-7,77671-22-8
acetic acid

: 1442445-64-8
(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

Guidance literature:: With hydrogenchloride; iron; In ethanol; water; at 90 ℃; for 0.75h;

Reference yield:

: 1442445-20-6
(S)-N-((R)-1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-2-methylpropane-2-sulfinamide

: 1442445-64-8
(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol; 1,4-dioxane / 0.5 h / 20 °C

2: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

3: hydrogenchloride; iron / ethanol; water / 0.75 h / 90 °C

With hydrogenchloride; iron; potassium carbonate; In 1,4-dioxane; methanol; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 320-43-4
4-chloro-2-(trifluoromethyl)benzaldehyde

: 1442445-64-8
(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: titanium(IV) tetraethanolate / dichloromethane / 48 h / 20 °C

2: dichloromethane; diethyl ether / 18 h / -48 °C

3: hydrogenchloride / methanol; 1,4-dioxane / 0.5 h / 20 °C

4: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

5: hydrogenchloride; iron / ethanol; water / 0.75 h / 90 °C

With hydrogenchloride; titanium(IV) tetraethanolate; iron; potassium carbonate; In 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide;