C₂₅H₃₁N₇O₅S

Base Information

Chemical Name:C₂₅H₃₁N₇O₅S
CAS No.:1542268-03-0
Molecular Formula:C₂₅H₃₁N₇O₅S
Molecular Weight:541.631
Hs Code.:

C<sub>25</sub>H<sub>31</sub>N<sub>7</sub>O<sub>5</sub>S

Synonyms:C₂₅H₃₁N₇O₅S

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Chemical Property of C₂₅H₃₁N₇O₅S

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Technology Process of C₂₅H₃₁N₇O₅S

There total 13 articles about C₂₅H₃₁N₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 350595-57-2
(S)-3-methylmorpholine

: 1542268-02-9
C₂₇H₂₈N₆O₆S₂

: 1542268-03-0
C₂₅H₃₁N₇O₅S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 90 ℃; for 0.5h; Microwave irradiation;

Reference yield:

: 2345-34-8
4-acetyloxy-benzoic acid

: 1542268-03-0
C₂₅H₃₁N₇O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride / 4 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

3.1: potassium carbonate / methanol / 5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 4 °C / Inert atmosphere

4.2: 3 h / 20 °C / Inert atmosphere

5.1: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.5 h / 90 °C / Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 99-96-7
4-hydroxy-benzoic acid

: 1542268-03-0
C₂₅H₃₁N₇O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / 4 h / 20 °C

2.1: oxalyl dichloride / 4 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

4.1: potassium carbonate / methanol / 5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 4 °C / Inert atmosphere

5.2: 3 h / 20 °C / Inert atmosphere

6.1: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.5 h / 90 °C / Microwave irradiation

With pyridine; bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;