2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine

Base Information

• Chemical Name: 2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine
• CAS No.: 1054633-01-0
• Molecular Formula: C₄₅H₄₆N₂O₁₁S
• Molecular Weight: 822.933

Synonyms:2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine

Chemical Property of 2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine

Chemical Property:

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Technology Process of 2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine

There total 1 articles about 2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2,4,6-triisopropylphenylsulfonyl chloride (6553-96-4) + tribenzoyl uridine (1748-04-5) → 2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine (1054633-01-0)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 10h; cooling;

DOI:10.1021/jo0617666

Reference yield: 88.0%

2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine (1054633-01-0) + benzyl 2-(dimethoxyphosphoryl)acetate (57443-18-2) → C41H37N2O13P

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 4.5h; cooling;

DOI:10.1021/jo0617666

Reference yield: 83.0%

2',3',5'-tris(O-benzoyl)-4-O-[(2,4,6-triisopropylphenyl)sulfonyl]uridine (1054633-01-0) + tert-butyl dimethylphosphonoacetate (62327-21-3) → C38H39N2O13P (918299-61-3)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 7.5h; cooling;

DOI:10.1021/jo0617666

upstream raw materials:

2,4,6-triisopropylphenylsulfonyl chloride

tribenzoyl uridine

Downstream raw materials:

C₃₈H₃₉N₂O₁₃P

{1-[3,4-bis(benzoyloxy)-5-(benzoyloxymethyl)tetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidene}methylphosphonic acid dimethyl ester

[difluoro{1-[3,4-bis(benzoyloxy)-5-(benzoyloxymethyl)tetrahydrofuran-2-yl]-2-oxo-1,2-dihydropyrimidin-4-yl}methyl]phosphonic acid dimethyl ester

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