3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

Base Information

Chemical Name:3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate
CAS No.:120383-99-5
Molecular Formula:C₂₀H₂₄O₃
Molecular Weight:312.409
Hs Code.:

Synonyms:3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

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Chemical Property of 3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

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Technology Process of 3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

There total 3 articles about 3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 563-79-1
2,3-Dimethyl-2-butene

: 15222-36-3
Benzoesaeure-α-chlorbenzylester

: 120383-99-5
3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

Guidance literature:: 2,3-Dimethyl-2-butene; Benzoesaeure-α-chlorbenzylester; With tin(IV) chloride; In nitromethane; at -10 - 20 ℃; for 1h;

With water; In diethyl ether;

Reference yield:

: 100-52-7
benzaldehyde

: 120383-99-5
3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ZnCl₂ / nitromethane / 1 h / -5 - 0 °C

2.1: SnCl₄ / nitromethane / 1 h / -10 - 20 °C

2.2: 81 percent / H₂O / diethyl ether

With tin(IV) chloride; zinc(II) chloride; In nitromethane; 1.1: Addition / 2.1: Addition / 2.2: Hydrolysis;

Reference yield:

: 98-88-4
benzoyl chloride

: 120383-99-5
3-hydroxy-1-phenyl-2,2,3-trimethylbutyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ZnCl₂ / nitromethane / 1 h / -5 - 0 °C

2.1: SnCl₄ / nitromethane / 1 h / -10 - 20 °C

2.2: 81 percent / H₂O / diethyl ether

With tin(IV) chloride; zinc(II) chloride; In nitromethane; 1.1: Addition / 2.1: Addition / 2.2: Hydrolysis;