N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

Base Information

Chemical Name:N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide
CAS No.:155826-73-6
Molecular Formula:C₂₀H₂₄BrNO₅
Molecular Weight:438.318
Hs Code.:

Synonyms:N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

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Chemical Property of N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

Chemical Property:

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Technology Process of N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

There total 9 articles about N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 104421-97-8
2-bromo-3,4-dimethoxyphenylacetyl chloride

: 155826-73-6
N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

Guidance literature:: In pyridine; benzene; at 20 ℃;
DOI:10.1021/jo982451w

Reference yield:

: 72912-39-1
(2-bromo-3,4-dimethoxyphenyl)acetonitrile

: 155826-73-6
N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 4N NaOH / ethanol / 20 h / Heating

2: SOCl₂ / benzene / 2 h / 50 - 60 °C

3: 91 percent / benzene; pyridine / 20 °C

With sodium hydroxide; thionyl chloride; In pyridine; ethanol; benzene; 1: Hydrolysis / 2: Substitution / 3: Acylation;
DOI:10.1021/jo982451w

Reference yield:

: 72912-38-0
(2-bromo-3,4-dimethoxyphenyl)methanol

: 155826-73-6
N-[2-[1-(3,4-dimethoxyphenyl)]ethyl]-2-bromo-3,4-dimethoxyphenylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / benzene / 20 °C

2: dimethylsulfoxide; benzene / 2 h

3: 92 percent / 4N NaOH / ethanol / 20 h / Heating

4: SOCl₂ / benzene / 2 h / 50 - 60 °C

5: 91 percent / benzene; pyridine / 20 °C

With sodium hydroxide; thionyl chloride; In pyridine; ethanol; dimethyl sulfoxide; benzene; 1: Substitution / 2: Substitution / 3: Hydrolysis / 4: Substitution / 5: Acylation;
DOI:10.1021/jo982451w