Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Base Information

Chemical Name:Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester
CAS No.:62774-38-3
Molecular Formula:C₁₅H₂₀O₇S
Molecular Weight:344.386
Hs Code.:

Synonyms:Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Suppliers and Price of Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

There total 7 articles about Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2873-28-1,2880-99-1,63069-63-6,76222-06-5,76222-07-6,96149-65-4,96192-31-3
Acetic acid (2R,3R,4S)-4-acetoxy-2-acetoxymethyl-5-bromo-6-methoxy-tetrahydro-pyran-3-yl ester

: 62774-38-3
Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CH₃ONa

2: H₂ / Ni(Raney)

3: TSOH

4: pyridine

With hydrogen; sodium methylate; toluene-4-sulfonic acid; Ni(Raney); In pyridine;
DOI:10.1016/S0040-4039(00)93163-0

Reference yield:

: 714276-13-8
methyl 2-bromo-2-deoxy-D-glucoside

: 62774-38-3
Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Ni(Raney)

2: TSOH

3: pyridine

With hydrogen; toluene-4-sulfonic acid; Ni(Raney); In pyridine;
DOI:10.1016/S0040-4039(00)93163-0

Reference yield:

: 2873-29-2
D-glucal triacetate

: 62774-38-3
Methanesulfonic acid (4aR,6R,8R,8aR)-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: N-brom-succinimide

2: CH₃ONa

3: H₂ / Ni(Raney)

4: TSOH

5: pyridine

With N-Bromosuccinimide; hydrogen; sodium methylate; toluene-4-sulfonic acid; Ni(Raney); In pyridine;
DOI:10.1016/S0040-4039(00)93163-0