(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Base Information

Chemical Name:(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate
CAS No.:258876-16-3
Molecular Formula:C₃₃H₂₈NO₆PS
Molecular Weight:597.628
Hs Code.:

Synonyms:(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Suppliers and Price of (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

There total 5 articles about (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3696-28-4
2,2'-dipyridyl disulfide bis-N-oxide

: 3-(diphenoxy-phosphoryloxy)-2-methyl-2,3-diphenyl-propionic acid

: 258876-16-3
(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Guidance literature:: With tributylphosphine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo991570o

Reference yield:

: 100-52-7
benzaldehyde

: 258876-16-3
(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi; hexamethyldisilamine / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -78 - -20 °C

2.1: CAN / acetonitrile; H₂O / 1 h / 20 °C

3.1: n-Bu₃P / CH₂Cl₂ / 20 °C

With n-butyllithium; ammonium cerium(IV) nitrate; tributylphosphine; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; dichloromethane; water; acetonitrile; 1.1: aldol condensation / 1.2: phosphorylation / 2.1: oxidative cleavage / 3.1: Esterification;
DOI:10.1021/jo991570o

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 258876-16-3
(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi; hexamethyldisilamine / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -78 - -20 °C

2.1: CAN / acetonitrile; H₂O / 1 h / 20 °C

3.1: n-Bu₃P / CH₂Cl₂ / 20 °C

With n-butyllithium; ammonium cerium(IV) nitrate; tributylphosphine; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; dichloromethane; water; acetonitrile; 1.1: aldol condensation / 1.2: phosphorylation / 2.1: oxidative cleavage / 3.1: Esterification;
DOI:10.1021/jo991570o