2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Base Information

Chemical Name:2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate
CAS No.:258876-13-0
Molecular Formula:C₃₇H₃₅O₈P
Molecular Weight:638.654
Hs Code.:

Synonyms:2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

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Chemical Property of 2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Chemical Property:

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Technology Process of 2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

There total 1 articles about 2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 2,4-dimethoxybenzyl 2-phenylpropanoate

: 258876-13-0
2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

Guidance literature:: benzaldehyde; 2,4-dimethoxybenzyl 2-phenylpropanoate; With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; at -78 ℃;

chlorophosphoric acid diphenyl ester; In tetrahydrofuran; at -78 - -20 ℃; Further stages.;
DOI:10.1021/jo991570o

Reference yield:

: 258876-13-0
2,4-dimethoxybenzyl 3-(diphenylphosphatoxy)-2-methyl-2,3-diphenylpropanoate

: 833-81-8,1017-22-7,34473-62-6,85165-70-4,779-51-1
1,2-diphenylpropene

Guidance literature:: Multi-step reaction with 3 steps

1: CAN / acetonitrile; H₂O / 1 h / 20 °C

2: n-Bu₃P / CH₂Cl₂ / 20 °C

3: 85 percent / t-BuSH; allyl alcohol / 1 h / 20 °C / Photolysis

With ammonium cerium(IV) nitrate; tributylphosphine; 2-methylpropan-2-thiol; allyl alcohol; In dichloromethane; water; acetonitrile; 1: oxidative cleavage / 2: Esterification / 3: Elimination;
DOI:10.1021/jo991570o