Technology Process of lavanducyanin
There total 7 articles about lavanducyanin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 0.23 h / 20 °C
2: oxygen / isopropyl alcohol / 24 h / 20 °C / Darkness
With
oxygen; potassium carbonate;
In
N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/acs.orglett.9b02601
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / mineral oil; dimethyl sulfoxide / 24 h / 20 °C
2: pyridine; trifluorormethanesulfonic acid / tetrahydrofuran / 1.5 h / 40 °C
3: pyridine; phosphorus tribromide / diethyl ether / 2.5 h / -78 - 20 °C
4: potassium carbonate / N,N-dimethyl-formamide / 0.23 h / 20 °C
5: oxygen / isopropyl alcohol / 24 h / 20 °C / Darkness
With
pyridine; trifluorormethanesulfonic acid; oxygen; phosphorus tribromide; sodium hydride; potassium carbonate;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol; mineral oil;
1: |Corey-Tschaikosky Epoxidation;
DOI:10.1021/acs.orglett.9b02601
