(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

Base Information

Chemical Name:(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester
CAS No.:213474-87-4
Molecular Formula:C₂₁H₂₅ClN₂O₅S
Molecular Weight:452.959
Hs Code.:

Synonyms:(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

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Technology Process of (S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

There total 3 articles about (S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 67-56-1
methanol

: 213474-81-8
(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

: 213474-87-4
(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

Guidance literature:: With thionyl chloride; for 4h; Ambient temperature;
DOI:10.1080/10426509708031609

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 213474-87-4
(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Et₃N, H₂O / tetrahydrofuran / 2 h / 20 °C

2: 50 percent / SOCl₂ / 4 h / Ambient temperature

With thionyl chloride; water; triethylamine; In tetrahydrofuran;
DOI:10.1080/10426509708031609

Reference yield:

: 126571-88-8
N-(4-chlorosulfonylphenylmethyl)-4-chlorobenzamide

: 213474-87-4
(S)-2-{4-[(4-Chloro-benzoylamino)-methyl]-benzenesulfonylamino}-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Et₃N, H₂O / tetrahydrofuran / 2 h / 20 °C

2: 50 percent / SOCl₂ / 4 h / Ambient temperature

With thionyl chloride; water; triethylamine; In tetrahydrofuran;
DOI:10.1080/10426509708031609