methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Base Information

Chemical Name:methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate
CAS No.:1454711-12-6
Molecular Formula:C₂₄H₃₂O₆
Molecular Weight:416.514
Hs Code.:

Synonyms:methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

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Technology Process of methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

There total 8 articles about methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1454711-11-5
methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

: 333-27-7
methyl trifluoromethanesulfonate

: 1454711-12-6
methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Guidance literature:: With 2,6-di-tert-butyl-pyridine; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2013.05.153

Reference yield:

: 1454711-09-1
(4S)-3-((2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoyl)-4-isopropyloxazolidin-2-one

: 1454711-12-6
methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

1.2: 1 h / 0 °C

2.1: 2,6-di-tert-butyl-pyridine / dichloromethane / 12 h / 0 - 20 °C

With 2,6-di-tert-butyl-pyridine; dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.05.153

Reference yield:

: 5673-98-3
2-methylpent-4-en-1-ol

: 1454711-12-6
methyl (2S,3S)-2-(benzyloxy)-3-methoxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran

2.1: dichloromethane / -78 °C / Cooling with acetone-dry ice

3.1: triethylamine; tin(II) trifluoromethanesulfonate / dichloromethane / 1 h / -78 °C

4.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

4.2: 1 h / 0 °C

5.1: 2,6-di-tert-butyl-pyridine / dichloromethane / 12 h / 0 - 20 °C

With tin(II) trifluoromethanesulfonate; 2,6-di-tert-butyl-pyridine; dihydrogen peroxide; sodium hydride; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.05.153