methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Base Information

Chemical Name:methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate
CAS No.:1454711-11-5
Molecular Formula:C₂₃H₃₀O₆
Molecular Weight:402.488
Hs Code.:

Synonyms:methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

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Chemical Property of methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

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Technology Process of methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

There total 7 articles about methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1454711-09-1
(4S)-3-((2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoyl)-4-isopropyloxazolidin-2-one

: 1454711-11-5
methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Guidance literature:: (4S)-3-((2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoyl)-4-isopropyloxazolidin-2-one; With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 3h;

diazomethane; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2013.05.153

Reference yield:

: 5673-98-3
2-methylpent-4-en-1-ol

: 1454711-11-5
methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran

2.1: dichloromethane / -78 °C / Cooling with acetone-dry ice

3.1: triethylamine; tin(II) trifluoromethanesulfonate / dichloromethane / 1 h / -78 °C

4.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

4.2: 1 h / 0 °C

With tin(II) trifluoromethanesulfonate; dihydrogen peroxide; sodium hydride; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.05.153

Reference yield:

: 1322762-83-3
1-methoxy-4-[(2-methylpent-4-enyloxy)methyl]benzene

: 1454711-11-5
methyl (2S,3S)-2-(benzyloxy)-3-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / -78 °C / Cooling with acetone-dry ice

2.1: triethylamine; tin(II) trifluoromethanesulfonate / dichloromethane / 1 h / -78 °C

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

3.2: 1 h / 0 °C

With tin(II) trifluoromethanesulfonate; dihydrogen peroxide; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.05.153