potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Base Information

Chemical Name:potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate
CAS No.:1200445-82-4
Molecular Formula:C₂₄H₂₁ClNO₄*K
Molecular Weight:461.986
Hs Code.:

Synonyms:potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

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Chemical Property of potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

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Technology Process of potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

There total 11 articles about potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-22-3
2-methyl-5-hydroxybenzoic acid

: 1200445-82-4
potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C

2: water; lithium hydroxide / 1,4-dioxane / 20 °C / Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: hydrogenchloride; water; acetic acid / 2 h / 90 °C

6: potassium hydroxide / methanol; water / 20 °C

With hydrogenchloride; oxalyl dichloride; water; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; potassium hydroxide; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

: 1200445-82-4
potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: With potassium hydroxide; In methanol; water; at 20 ℃;

Reference yield:

: 446-33-3
5-Fluoro-2-nitrotoluene

: 1200445-82-4
potassium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Cooling with ice

1.2: 88 h / 20 - 100 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr

3.1: triethylamine / dichloromethane / 20 °C

4.1: hydrogenchloride; water; acetic acid / 2 h / 90 °C

5.1: potassium hydroxide / methanol; water / 20 °C

With hydrogenchloride; water; hydrogen; sodium hydride; acetic acid; triethylamine; potassium hydroxide; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;