[3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide

Base Information

Chemical Name:[3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide
CAS No.:855249-37-5
Molecular Formula:Br*C₃₇H₃₃FN₂P
Molecular Weight:635.559
Hs Code.:

Synonyms:[3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide

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Chemical Property of [3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide

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Technology Process of [3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide

There total 1 articles about [3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 855249-35-3
[3-(4-fluorophenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-yl]methanol

: 6399-81-1
triphenylphosphine hydrobromide

: 855249-37-5
[3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide

Guidance literature:: [3-(4-fluorophenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-yl]methanol; triphenylphosphine hydrobromide; With hydrogenchloride; In diethyl ether; dichloromethane; at 25 ℃; for 1h;

With sodium hydrogencarbonate; In diethyl ether; dichloromethane; water;

Reference yield: 66.0%

: 855249-37-5
[3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide

: 124752-23-4
tert-butyl 2-[(4R,6S)-6-formyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate

: ((4R,6S)-6-{2-[3-(4-fluorophenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-yl]vinyl}-2,2-dimethyl[1,3]dioxan-4-yl)acetic acid tert-butyl ester

Guidance literature:: [3-(4-fluoro-phenyl)-1-isopropyl-4-pyridin-2-yl-1H-pyrrol-2-ylmethyl]-triphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; at -78 ℃; for 0.0833333h;

tert-butyl 2-[(4R,6S)-6-formyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate; In tetrahydrofuran; dimethyl sulfoxide; at -78 - 25 ℃; for 2h;

With ammonium chloride; In tetrahydrofuran; water; dimethyl sulfoxide;