Dibenzo(c,mno)chrysene

Base Information

• Chemical Name: Dibenzo(c,mno)chrysene
• CAS No.: 196-28-1
• Molecular Formula: C24H14
• Molecular Weight: 302.375
• Hs Code.: 2902909090
• European Community (EC) Number: 205-897-4
• DSSTox Substance ID: DTXSID80173261
• Nikkaji Number: J193.673E
• Wikidata: Q83043325
• Mol file: 196-28-1.mol

Synonyms:DB(C,mno)C;dibenzo(c,mno)chrysene

Chemical Property of Dibenzo(c,mno)chrysene

Chemical Property:

• Vapor Pressure: 1.12E-11mmHg at 25°C
• Boiling Point: 552.3°Cat760mmHg
• Flash Point: 282°C
• PSA: 0.00000
• Density: 1.313g/cm³
• LogP: 6.89040
• XLogP3: 7.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 302.109550447
• Heavy Atom Count: 24
• Complexity: 480

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC3=CC4=C5C(=C32)C=CC6=CC=CC(=C65)C=C4

Technology Process of Dibenzo(c,mno)chrysene

There total 8 articles about Dibenzo(c,mno)chrysene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-[2-(β-methoxyethenyl)phenyl]pyrene → Dibenzo[c,mno]chrysene (196-28-1)

Guidance literature:

With methanesulfonic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/tx0200111

Reference yield: 69.0%

5-(β-methoxyethenyl)benzo[c]chrysene → Dibenzo[c,mno]chrysene (196-28-1)

Guidance literature:

With methanesulfonic acid; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/tx0200111

Reference yield: 52.0%

C30H20 (1146542-52-0) → Dibenzo[c,mno]chrysene (196-28-1)

Guidance literature:

With trifluorormethanesulfonic acid; In CH₃Cl; at 25 ℃;

DOI:10.1016/j.tetlet.2009.02.042

upstream raw materials:

Perinaphthenon

(2-methyl-1-naphthyl)magnesium bromide

1-bromopyrene

2-formylbenzene boronic acid

Refernces

• 1、 Desai, Dhimant,Sharma, Arun K.,Lin, Jyh-Ming,Krzeminski, Jacek,Pimentel, Maria,El-Bayoumy, Karam,Nesnow, Stephen,Amin, Shantu. "Synthesis, in vitro metabolism, cell transformation, mutagenicity, and DNA adduction of dibenzo[c,mno] chrysene". . p. 964 - 971. Retrieved 2008/04/18.