[1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

Base Information

Chemical Name:[1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester
CAS No.:130882-60-9
Molecular Formula:C₁₄H₂₂Cl₂NO₃P
Molecular Weight:354.213
Hs Code.:

Synonyms:[1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

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Chemical Property of [1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

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Technology Process of [1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

There total 3 articles about [1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.4%

: 130829-05-9
(2-(2,3-Dichloro-phenyl)-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphonic acid diisopropyl ester

: 130882-60-9
[1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In isopropyl alcohol; at 20 - 25 ℃; for 19h;

Reference yield:

: 32768-54-0
2,3-dichlorotoluene

: 130882-60-9
[1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NBS / AIBN / CCl₄

2: 1) LDA / 1) THF, - 75 deg C, 1 h, 2) overnight, r.t.

3: 90.4 percent / H₂ / Pd/C (5percent Pd) / propan-2-ol / 19 h / 20 - 25 °C

With N-Bromosuccinimide; hydrogen; lithium diisopropyl amide; 2,2'-azobis(isobutyronitrile); 5%-palladium/activated carbon; In tetrachloromethane; isopropyl alcohol;

Reference yield:

: 57915-78-3
1-(bromomethyl)-2,3-dichlorobenzene

: 130882-60-9
[1-Amino-2-(2,3-dichloro-phenyl)-ethyl]-phosphonic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / 1) THF, - 75 deg C, 1 h, 2) overnight, r.t.

2: 90.4 percent / H₂ / Pd/C (5percent Pd) / propan-2-ol / 19 h / 20 - 25 °C

With hydrogen; lithium diisopropyl amide; 5%-palladium/activated carbon; In isopropyl alcohol;