(2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

Base Information

Chemical Name:(2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester
CAS No.:719307-95-6
Molecular Formula:C₂₂H₂₄N₂O₆
Molecular Weight:412.442
Hs Code.:

Synonyms:(2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

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Chemical Property of (2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

Chemical Property:

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Technology Process of (2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

There total 5 articles about (2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₆ClNO₅

: 613-89-8
2-Aminoacetophenone

: 719307-95-6
(2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h;

Reference yield:

: (S)-2-Benzyloxycarbonylamino-succinic acid 1-ethyl ester; compound with dicyclohexyl-amine

: 719307-95-6
(2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; water / diethyl ether / 18 h / Heating / reflux

2: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 18 h / 20 °C

3: triethylamine / dichloromethane / 4 h / 0 - 20 °C

With thionyl chloride; sulfuric acid; water; triethylamine; N,N-dimethyl-formamide; In diethyl ether; dichloromethane;

Reference yield:

: 4668-43-3
(S)-3-(benzyloxycarbonylamino)-4-ethoxy-4-oxobutanoic acid

: 719307-95-6
(2S)-2-benzyloxycarbonylamino-N-(2-oxo-2-phenyl-ethyl)-succinamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 18 h / 20 °C

2: triethylamine / dichloromethane / 4 h / 0 - 20 °C

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;