(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

Base Information

Chemical Name:(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride
CAS No.:719308-31-3
Molecular Formula:C₁₄H₁₆N₂O₃*ClH
Molecular Weight:296.754
Hs Code.:

Synonyms:(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

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Chemical Property of (2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

Chemical Property:

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Technology Process of (2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

There total 7 articles about (2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 755753-54-9
(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester

: 719308-31-3
(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether;

Reference yield:

: (S)-2-Benzyloxycarbonylamino-succinic acid 1-ethyl ester; compound with dicyclohexyl-amine

: 719308-31-3
(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid; water / diethyl ether / 18 h / Heating / reflux

2: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 18 h / 20 °C

3: triethylamine / dichloromethane / 4 h / 0 - 20 °C

4: trichlorophosphate / toluene / 1.5 h / 100 °C

5: hydrogen bromide; acetic acid / 1 h / 20 °C

6: hydrogenchloride / diethyl ether

With hydrogenchloride; thionyl chloride; sulfuric acid; water; hydrogen bromide; acetic acid; triethylamine; trichlorophosphate; N,N-dimethyl-formamide; In diethyl ether; dichloromethane; toluene;

Reference yield:

: 4668-43-3
(S)-3-(benzyloxycarbonylamino)-4-ethoxy-4-oxobutanoic acid

: 719308-31-3
(2S)-2-amino-3-(5-phenyl-oxazol-2-yl)-propionic acid ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 18 h / 20 °C

2: triethylamine / dichloromethane / 4 h / 0 - 20 °C

3: trichlorophosphate / toluene / 1.5 h / 100 °C

4: hydrogen bromide; acetic acid / 1 h / 20 °C

5: hydrogenchloride / diethyl ether

With hydrogenchloride; thionyl chloride; hydrogen bromide; acetic acid; triethylamine; trichlorophosphate; N,N-dimethyl-formamide; In diethyl ether; dichloromethane; toluene;