cyclobutylphenyldiazomethane

Base Information

• Chemical Name: cyclobutylphenyldiazomethane
• CAS No.: 82517-28-0
• Molecular Formula: C₁₁H₁₂N₂
• Molecular Weight: 172.23
• Mol file: 82517-28-0.mol

Synonyms:cyclobutylphenyldiazomethane

Chemical Property of cyclobutylphenyldiazomethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclobutylphenyldiazomethane

There total 1 articles about cyclobutylphenyldiazomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.7%

cyclobutyl phenyl ketone (p-toluenesulfonyl)hydrazone sodium salt → cyclobutylphenyldiazomethane (82517-28-0)

Guidance literature:

under 0.01 Torr; Heating;

DOI:10.1021/ja00072a014

Reference yield:

cyclobutylphenyldiazomethane (82517-28-0) → cyclobutylphenylcarbene (82517-40-6)

Guidance literature:

In 2-methyltetrahydrofuran; at -263.2 - -248.2 ℃; Irradiation;

DOI:10.1016/S0040-4039(00)87094-X

Reference yield:

methanol (67-56-1) + cyclobutylphenyldiazomethane (82517-28-0) → cyclopent-1-en-1-ylbenzene (825-54-7) + benzylidenecyclobutane (5244-75-7) + cyclobutylphenylmethyl methyl ether

Guidance literature:

Product distribution; Mechanism; Irradiation; other alkyl aryl diazo compounds; also in the pyridine;

DOI:10.1021/ja00072a014

Downstream raw materials:

cyclopent-1-en-1-ylbenzene

benzylidenecyclobutane

cyclobutylphenylcarbene