N_.N-Bis-trimethylsilyl-p-cyanoanilin

Base Information

Chemical Name:N_.N-Bis-trimethylsilyl-p-cyanoanilin
CAS No.:31945-23-0
Molecular Formula:C₁₃H₂₂N₂Si₂
Molecular Weight:262.502
Hs Code.:

N<sub>.</sub>N-Bis-trimethylsilyl-p-cyanoanilin

Synonyms:N_.N-Bis-trimethylsilyl-p-cyanoanilin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N_.N-Bis-trimethylsilyl-p-cyanoanilin

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Technology Process of N_.N-Bis-trimethylsilyl-p-cyanoanilin

There total 4 articles about N_.N-Bis-trimethylsilyl-p-cyanoanilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: bis(bis(trimethylsilyl)amido)zinc(II)

: 623-00-7
4-bromobenzenecarbonitrile

: 31945-23-0
N_.N-Bis-trimethylsilyl-p-cyanoanilin

Guidance literature:: With tri-tert-butyl phosphine; lithium chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 50 ℃; for 3h; Further Variations:; Reagents; Solvents; times; Product distribution;
DOI:10.1021/ol050141b

Reference yield:

: 13032-12-7
1,1'-bis(trimethylsilyl)-1,1',4,4'-tetrahydro-4,4'-bipyridylidene

: 619-72-7
4-nitrobenzonitrile

: 31945-23-0
N_.N-Bis-trimethylsilyl-p-cyanoanilin

Guidance literature:: 1,1'-bis(trimethylsilyl)-1,1',4,4'-tetrahydro-4,4'-bipyridylidene; 4-nitrobenzonitrile; In acetonitrile; Schlenk technique; Glovebox; Inert atmosphere;

With dibenzothiophene; In acetonitrile; at 100 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201801972