(2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

Base Information

Chemical Name:(2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester
CAS No.:1203586-50-8
Molecular Formula:C₁₈H₁₇N₃O₄
Molecular Weight:339.351
Hs Code.:

Synonyms:(2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

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Chemical Property of (2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

Chemical Property:

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Technology Process of (2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

There total 3 articles about (2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1203586-29-1
C₁₇H₁₅N₃O₄

: 1203586-50-8
(2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

Guidance literature:: With thionyl chloride; at 0 ℃;
DOI:10.1039/c1ob06304a

Reference yield:

: 73-22-3,27732-43-0,80206-30-0,27813-82-7
L-Tryptophan

: 1203586-50-8
(2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 25 - 90 °C

2: thionyl chloride / 0 °C

With thionyl chloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c1ob06304a

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1203586-50-8
(2S)-3-(1H-indol-3-yl)-2-(2-nitrophenylamino)propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 25 - 90 °C

2: thionyl chloride / 0 °C

With thionyl chloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c1ob06304a