(dipicolinate)V(O)(α-tert-butylbenzylalkoxide)

Base Information

Chemical Name:(dipicolinate)V(O)(α-tert-butylbenzylalkoxide)
CAS No.:1259331-50-4
Molecular Formula:C₁₈H₁₈NO₆V
Molecular Weight:395.286
Hs Code.:

Synonyms:(dipicolinate)V(O)(α-tert-butylbenzylalkoxide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (dipicolinate)V(O)(α-tert-butylbenzylalkoxide)

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Technology Process of (dipicolinate)V(O)(α-tert-butylbenzylalkoxide)

There total 1 articles about (dipicolinate)V(O)(α-tert-butylbenzylalkoxide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 172615-09-7
dipicolinate vanadium(V) isopropoxide

: 3835-64-1
2,2-dimethyl-1-phenylpropan-1-ol

: 1259331-50-4
(dipicolinate)V(O)(α-tert-butylbenzylalkoxide)

Guidance literature:: With calcium hydride; In acetonitrile; (Ar) α-tertbutylbenzyl alcohol and CaH2 were stirred in MeCN for 3h, soln. was filtered to vial with V complex, stirred at room temp. for 20 min; solvent was removed in vacuo, MeCN was added, stirred at room temp. for 20 min, solvent was evapd. in vacuo, Et2O was added, mixt. was stirred for 2 h at room temp., solid was collected, washed with Et2O, dried in vacuo;
DOI:10.1021/ja105739k