methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride

Base Information

• Chemical Name: methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride
• CAS No.: 1236000-51-3
• Molecular Formula: C₉H₁₀F₃NO*ClH
• Molecular Weight: 241.641

Synonyms:methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride

Chemical Property of methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

N-Methyl-1-(4-(trifluoromethoxy)phenyl)methanaminehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride

There total 1 articles about methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

p-trifluoromethoxybenzaldehyde (659-28-9) + methylamine (74-89-5) → methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride (1236000-51-3)

Guidance literature:

p-trifluoromethoxybenzaldehyde; methylamine; With sodium tetrahydroborate; In methanol; water; at 0 - 20 ℃;

With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 0 ℃;

Reference yield: 91.0%

5-bromo-1-benzothiophene-2-carboxylic acid (7312-10-9) + methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride (1236000-51-3) → 5-bromo-N-methyI-N-({4-[(trifluoromethyl)oxy]phenyl}methyl)-1-benzothiophene-2-carboxamide (1236000-73-9)

Guidance literature:

With O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield: 91.0%

methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride (1236000-51-3) + 3-Iodobenzoic acid (618-51-9) → 3-iodo-N-methyI-N-({4-[(trifluoromethyl)oxy]phenyl}methyl)benzamide (1236000-72-8)

Guidance literature:

3-Iodobenzoic acid; With dicyclohexyl-carbodiimide; In dichloromethane; for 1h; Inert atmosphere;

methyl({4-[(trifluoromethyl)oxy]phenyl}methyl)amine hydrochloride; With triethylamine; In dichloromethane;

upstream raw materials:

p-trifluoromethoxybenzaldehyde

methylamine

Downstream raw materials:

3-butyn-1-yl(methyl)({4-[(trifluoromethyl)oxy]phenyl}methyl)amine

3-iodo-N-methyI-N-({4-[(trifluoromethyl)oxy]phenyl}methyl)benzamide

5-bromo-N-methyI-N-({4-[(trifluoromethyl)oxy]phenyl}methyl)-1-benzothiophene-2-carboxamide

{[5-(4-bromophenyl)-2-thienyl]methyl}methyl({4[(trifluoromethyl)oxy]phenyl}methyl)amine

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