methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

Base Information

Chemical Name:methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate
CAS No.:191401-90-8
Molecular Formula:C₂₁H₃₂N₂O₆
Molecular Weight:408.495
Hs Code.:

Synonyms:methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

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Chemical Property of methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

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Technology Process of methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

There total 3 articles about methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 957494-09-6
3-benzyloxycarbonylamino-7-tert-butoxycarbonylamino-heptanoic acid

: 74-88-4
methyl iodide

: 191401-90-8
methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

Guidance literature:: In acetonitrile; at 20 ℃;

Reference yield: 80.0%

: 67-56-1
methanol

: 114479-97-9
(S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-1-diazoheptan-2-one

: 191401-90-8
methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

Guidance literature:: With silver benzoate; triethylamine; at -25 - 20 ℃; for 5h;
DOI:10.1002/hlca.200390133

Reference yield:

: 2389-60-8
Z-Lys(Boc)-OH

: 191401-90-8
methyl (S)-3-{[(benzyloxy)carbonyl]amino}-7-{[(tert-butoxy)carbonyl]amino}-heptanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N; i-BuOCOCl / tetrahydrofuran / 0.5 h / -25 °C

1.2: 74 percent / tetrahydrofuran; diethyl ether / 16 h

2.1: 80 percent / silver benzoate; Et₃N / 5 h / -25 - 20 °C

With silver benzoate; triethylamine; isobutyl chloroformate; In tetrahydrofuran;
DOI:10.1002/hlca.200390133