3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

Base Information

Chemical Name:3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine
CAS No.:133958-35-7
Molecular Formula:C₁₅H₂₀N₄O₃
Molecular Weight:304.349
Hs Code.:

Synonyms:3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

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Chemical Property of 3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

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Technology Process of 3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

There total 3 articles about 3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 133958-33-5
3,5-dimethyl-8-oxo-9-phenyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

: 133958-35-7
3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

Guidance literature:: With methylamine; In methanol; at 20 - 25 ℃; for 10h;
DOI:10.1007/BF00473969

Reference yield: 9.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 2152-34-3,3469-01-0
2-amino-5-phenyl-4-oxazolinone

: 74-89-5
methylamine

: 133958-35-7
3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

Guidance literature:: In methanol; water; at 30 ℃; for 4h;
DOI:10.1007/BF00473969

Reference yield:

: 2152-34-3,3469-01-0
2-amino-5-phenyl-4-oxazolinone

: 133958-35-7
3,5-dimethyl-8-oxo-9-phenyl-9-hydroxymethyl-2,3,4,5,6,7-hexahydrooxazolo-<3,2-a>-1,3,5,7-tetrazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 4 percent / formalin / methanol; H₂O / 6.5 h / 5 °C

2: 62 percent / 25percent aq.methylamine / methanol / 10 h / 20 - 25 °C

With formaldehyd; methylamine; In methanol; water;
DOI:10.1007/BF00473969