methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Base Information

Chemical Name:methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate
CAS No.:1356601-43-8
Molecular Formula:C₂₉H₃₁NO₅
Molecular Weight:473.569
Hs Code.:

Synonyms:methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Chemical Property of methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Technology Process of methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

There total 7 articles about methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.8%

: 1073545-90-0
3-cyclopropyl-3-(4-hydroxyphenyl)propanoic acid methyl ester

: 1356599-86-4
(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol

: 1356601-43-8
methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 15h;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356601-43-8
methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium acetate; acetic acid / 0.08 h / 20 °C

1.2: 3 h / 20 - 80 °C

2.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

2.2: 5 h / 20 - 80 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 15 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; sodium acetate; potassium carbonate; acetic acid; triphenylphosphine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1356601-43-8
methyl 3-cyclopropyl-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: water / 2 h / 75 °C

2.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C

3.1: water / N,N-dimethyl-formamide / 15 h / 90 °C

4.1: methanesulfonic acid / 2 h / 65 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 15 h / 0 - 20 °C

With methanesulfonic acid; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;