tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Base Information

Chemical Name:tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate
CAS No.:1237587-16-4
Molecular Formula:C₂₄H₂₄Cl₂F₃N₃O₄
Molecular Weight:546.373
Hs Code.:

Synonyms:tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

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Chemical Property of tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Chemical Property:

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Technology Process of tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

There total 11 articles about tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-14-2
tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 74-88-4
methyl iodide

: 1237587-16-4
tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Guidance literature:: tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃;

methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 10h;

Reference yield:

: tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 74-88-4
methyl iodide

: 1237587-16-4
tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Guidance literature:: tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 10h;

Reference yield:

: 3431-62-7,20747-39-1
3-nitrobenzaldoxime

: 1237587-16-4
tert-butyl N'-acetyl-N'-methyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: acetic acid; iron / ethanol; water / 1.25 h / 20 - 75 °C

3.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

4.1: 4-dimethylpyridine / tetrahydrofuran / 1.5 h / 20 °C

5.1: sodium hydroxide; sodium hypochlorite; ammonia; ammonium chloride / Aliquat 336 / water; tert-butyl methyl ether / 12.33 h / 20 °C

6.1: triethylamine / tetrahydrofuran / 14 h / 0 - 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

7.2: 10 h / 20 °C

With sodium hypochlorite; N-chloro-succinimide; ammonia; iron; sodium hydride; ammonium chloride; acetic acid; triethylamine; sodium hydroxide; Aliquat 336; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide; mineral oil;