benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)

Base Information

Chemical Name:benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)
CAS No.:120272-57-3
Molecular Formula:C₂H₆Cl₃OPtS*C₂₅H₂₂P
Molecular Weight:732.997
Hs Code.:

Synonyms:benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)

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Chemical Property of benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)

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Technology Process of benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)

There total 9 articles about benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 15274-33-6
cis-bis(dimethylsulfoxide)dichloroplatinum(II)

: 1100-88-5
benzyltriphenylphosphonium chloride

: 120272-57-3
triphenylbenzylphosphonium-Pt(dimethyl sulfoxide)Cl₃

Guidance literature:: In acetonitrile; addn. of org. ligand to suspn. of Pt-complex (20°C); solvent removal (vac., room temp.); oily residue crystn. under a layer of ethanol, ppt. filtered out, washed with ethanol and ether and air-dried (75°C); elem. anal.;

Reference yield: 94.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 1100-88-5
benzyltriphenylphosphonium chloride

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 120272-57-3
benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)

Guidance literature:: In dimethyl sulfoxide; byproducts: KCl; mixing Pt complex, P compd., DMSO, stirring at room temp. for 5 min; slow evapn., isolation of crystals, elem. anal.;
DOI:10.1134/S1070363210090057

Reference yield:

: 337526-25-7
(Ph₃PCH₂Ph)(PtCl₅(Me₂SO))

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 120272-57-3
benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)

: 2181-97-7
(2-methoxy-2-oxoethyl)triphenylphosphonium chloride

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: In dichloromethane; Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent;
DOI:10.1021/ic000769c