[2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Base Information

Chemical Name:[2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile
CAS No.:351459-67-1
Molecular Formula:C₁₈H₁₃IN₂
Molecular Weight:384.219
Hs Code.:

Synonyms:[2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Suppliers and Price of [2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

There total 4 articles about [2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 27081-10-3
tropylium tetrafluoroborate

: 351459-69-3
2[1-(4-iodophenyl)ethylidene]propanedinitrile

: 351459-67-1
[2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1002/1522-2675(20010418)84:4<743::AID-HLCA743>3.0.CO;2-1

Reference yield: 75.0%

: 109-77-3
malononitrile

: 351459-66-0
2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethanone

: 351459-67-1
[2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Guidance literature:: With ammonium acetate; In acetic acid; toluene; for 8h; Heating;
DOI:10.1002/1522-2675(20010418)84:4<743::AID-HLCA743>3.0.CO;2-1

Reference yield:

: 13329-40-3
4-Iodoacetophenone

: 351459-67-1
[2-(2,4,6-cycloheptatriene-1-yl)-1-(4-iodophenyl)ethylidene]propanedinitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / methanol; acetic acid / 6 h / 20 °C

2: 69 percent / NH₄OAc / toluene; acetic acid / 96 h / Heating

3: 100 percent / Et₃N / CH₂Cl₂ / 1 h / -78 °C

With ammonium acetate; triethylamine; In methanol; dichloromethane; acetic acid; toluene;
DOI:10.1002/1522-2675(20010418)84:4<743::AID-HLCA743>3.0.CO;2-1