(S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Base Information

Chemical Name:(S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester
CAS No.:1334513-04-0
Molecular Formula:C₁₈H₂₀ClN₂O₇P
Molecular Weight:442.793
Hs Code.:

Synonyms:(S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

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Chemical Property of (S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

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Technology Process of (S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

There total 4 articles about (S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (2S)-isopropyl 2-(((2-chloro-4-nitrophenoxy)(phenoxy)phosphoryl)amino)propanoate

: 1334513-06-2
(S)-2-[(R)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

: 1334513-04-0
(S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Guidance literature:: In hexane; ethyl acetate; at -20 ℃; for 16h;

Reference yield: 76.0%

: 619-08-9
2-chloro-4-nitrophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 39613-92-8,62062-56-0,62062-65-1
alanine isopropyl ester hydrochloride

: 1334513-06-2
(S)-2-[(R)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

: 1334513-04-0
(S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Guidance literature:: O-phenyl phosphorodichloridate; alanine isopropyl ester hydrochloride; With triethylamine; In dichloromethane; at -78 - 0 ℃; for 1.5h;

2-chloro-4-nitrophenol; With triethylamine; In dichloromethane; at 0 ℃; for 2.33333h;

Reference yield:

: 619-08-9
2-chloro-4-nitrophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 1334513-06-2
(S)-2-[(R)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

: 1334513-04-0
(S)-2-[(S)-(2-chloro-4-nitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.5 h / -78 - 0 °C

1.2: 2 h / 0 °C

2.1: hexane; ethyl acetate / 16 h / -20 °C

With triethylamine; In hexane; dichloromethane; ethyl acetate;