[5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine

Base Information

• Chemical Name: [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine
• CAS No.: 490035-85-3
• Molecular Formula: C₃₄H₂₇N₃O₂
• Molecular Weight: 509.607

Synonyms:[5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine

Chemical Property of [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine

Chemical Property:

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Technology Process of [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine

There total 4 articles about [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1‐(4‐methoxyphenyl)‐4‐nitro‐3‐phenylbutan‐1‐one (219607-58-6) → [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine (490035-85-3)

Guidance literature:

With ammonium acetate; In butan-1-ol; for 24h; Reflux;

DOI:10.2174/157017811796064377

Reference yield:

benzaldehyde (100-52-7) → [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine (490035-85-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol; water / 0.25 h / 0 °C

1.2: 24.25 h / 0 - 20 °C

2.1: alkaline hydroxide / ethanol / 12 h / 60 °C

3.1: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; sodium hydroxide; In ethanol; water; butan-1-ol; 2.1: Michael addition;

DOI:10.2174/157017811796064377

Reference yield:

4'-methoxychalcone (959-23-9) → [5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene]amine (490035-85-3)

Guidance literature:

Multi-step reaction with 2 steps

1: alkaline hydroxide / ethanol / 12 h / 60 °C

2: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; In ethanol; butan-1-ol; 1: Michael addition;

DOI:10.2174/157017811796064377

upstream raw materials:

1‐(4‐methoxyphenyl)‐4‐nitro‐3‐phenylbutan‐1‐one

benzaldehyde

4'-methoxychalcone

1-(4-methoxyphenyl)ethanone

Downstream raw materials:

[(5-(4-methoxyphenyl)-3-phenyl-1H-pyrrol-2-yl)(5-(4-methoxyphenyl)-3-phenylpyrrol-2-ylidene)amine]zinc

(triphenylphosphine)Ag(N(C₄HN(C₆H₅)C₆H₄OCH₃)2)

(triphenylphosphine)Cu(N(C₄HN(C₆H₅)C₆H₄OCH₃)2)

((C₆H₅)(C₆H₄OCH₃)C₄BrN)2NH

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