4-bromophenyl diethylcarbamate

Base Information

Chemical Name:4-bromophenyl diethylcarbamate
CAS No.:459408-70-9
Molecular Formula:C₁₁H₁₄BrNO₂
Molecular Weight:272.142
Hs Code.:

Synonyms:4-bromophenyl diethylcarbamate

Suppliers and Price of 4-bromophenyl diethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromophenyl diethylcarbamate

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Technology Process of 4-bromophenyl diethylcarbamate

There total 2 articles about 4-bromophenyl diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 617-84-5
N-formyldiethylamine

: 106-41-2
4-bromo-phenol

: 459408-70-9
4-bromophenyl diethylcarbamate

Guidance literature:: With tert.-butylhydroperoxide; 4,7-dimethoxy-1,10-phenanthroline; iron(II) bromide; In decane; at 60 ℃; for 4h; Inert atmosphere; Molecular sieve;
DOI:10.1080/00397911.2021.2017459

Reference yield: 68.0%

: 124-38-9,18923-20-1
carbon dioxide

: 5467-74-3
4-Bromophenylboronic acid

: 109-89-7
diethylamine

: 459408-70-9
4-bromophenyl diethylcarbamate

Guidance literature:: With pyridine; copper(I) oxide; boron trifluoride diethyl etherate; oxygen; In dichloromethane; at 80 ℃; for 24h; under 30003 Torr; Autoclave;
DOI:10.1039/c6gc03465a