4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

Base Information

Chemical Name:4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside
CAS No.:142329-90-6
Molecular Formula:C₂₆H₃₆N₂O₁₃
Molecular Weight:584.577
Hs Code.:

Synonyms:4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

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Chemical Property of 4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

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Technology Process of 4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

There total 2 articles about 4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64970-92-9
4-nitrophenyl 3,4-O-isopropylidene-β-D-galactopyranoside

: 142329-90-6
4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 41.5 percent / 4-toluenesulfonic acid monohydrate / 1,2-dichloro-ethane / 16 h / 70 °C

2: 1.) 0.01 M sodium methoxide, methanol, 2.) 4-toluenesulfonic acid monohydrate / 1.) r.t., 3 h, 2.) DMF, r.t., 16 h

With methanol; p-toluenesulfonic acid monohydrate; sodium methylate; In 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)90562-7

Reference yield:

: 142329-89-3
4-nitrophenyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopranosyl)-(1->6)-3,4-isopropylidene-β-D-galactopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 142329-90-6
4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: With methanol; p-toluenesulfonic acid monohydrate; sodium methylate; Yield given. Multistep reaction; 1.) r.t., 3 h, 2.) DMF, r.t., 16 h;
DOI:10.1016/S0008-6215(00)90562-7

Reference yield: 88.0%

: 98-88-4
benzoyl chloride

: 142329-90-6
4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopopylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

: 142329-91-7
4-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90562-7