Technology Process of C41H51N4O8PS
There total 10 articles about C41H51N4O8PS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-tetrazole; diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 4h;
DOI:10.1039/c1cc14339e
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 20 °C
2: tetraphosphorus decasulfide; potassium carbonate / toluene / 0.33 h / Reflux
3: (Z)-2-nitrobenzaldehyde oxime; N,N,N',N'-tetramethylguanidine / acetonitrile / 18 h / 20 °C
4: triethylamine tris(hydrogen fluoride); triethylamine / tetrahydrofuran / 1 h / 20 °C
5: pyridine / 6 h / 20 °C
6: 1H-tetrazole; diisopropylamine / dichloromethane / 4 h / 20 °C
With
pyridine; 1H-tetrazole; tetraphosphorus decasulfide; (Z)-2-nitrobenzaldehyde oxime; sodium hydride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; diisopropylamine; N,N,N',N'-tetramethylguanidine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1039/c1cc14339e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine tris(hydrogen fluoride); triethylamine / tetrahydrofuran / 1 h / 20 °C
2: pyridine / 6 h / 20 °C
3: 1H-tetrazole; diisopropylamine / dichloromethane / 4 h / 20 °C
With
pyridine; 1H-tetrazole; triethylamine tris(hydrogen fluoride); triethylamine; diisopropylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc14339e