C₁₇H₁₉Cl₂NO₄

Base Information

Chemical Name:C₁₇H₁₉Cl₂NO₄
CAS No.:1268246-45-2
Molecular Formula:C₁₇H₁₉Cl₂NO₄
Molecular Weight:372.248
Hs Code.:

C<sub>17</sub>H<sub>19</sub>Cl<sub>2</sub>NO<sub>4</sub>

Synonyms:C₁₇H₁₉Cl₂NO₄

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Chemical Property of C₁₇H₁₉Cl₂NO₄

Chemical Property:

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Technology Process of C₁₇H₁₉Cl₂NO₄

There total 8 articles about C₁₇H₁₉Cl₂NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1268246-44-1
C₁₉H₂₁Cl₂NO₅

: 1268246-45-2
C₁₇H₁₉Cl₂NO₄

Guidance literature:: C₁₉H₂₁Cl₂NO₅; With diisobutylaluminium hydride; In tetrahydrofuran; at -30 - 0 ℃; for 3.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran;

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 1268246-45-2
C₁₇H₁₉Cl₂NO₄

Guidance literature:: Multi-step reaction with 8 steps

1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 24 h / 90 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

3: sodium methylate / tetrahydrofuran / 16 h / 20 °C

4: N,N-dimethyl-formamide / 3 h / 110 °C

5: hydrogenchloride; silica gel / water; tetrahydrofuran / 1 h / 40 °C

6: sodium tetrahydroborate / ethanol / 0.33 h / 0 °C

7: toluene-4-sulfonic acid / dichloromethane / 20 °C / Inert atmosphere

8: diisobutylaluminium hydride / tetrahydrofuran / 3.5 h / -30 - 0 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; N-chloro-succinimide; hydroxylamine hydrochloride; sodium methylate; silica gel; diisobutylaluminium hydride; sodium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 25185-95-9
2,6-dichlorobenzaldoxime

: 1268246-45-2
C₁₇H₁₉Cl₂NO₄

Guidance literature:: Multi-step reaction with 7 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

2: sodium methylate / tetrahydrofuran / 16 h / 20 °C

3: N,N-dimethyl-formamide / 3 h / 110 °C

4: hydrogenchloride; silica gel / water; tetrahydrofuran / 1 h / 40 °C

5: sodium tetrahydroborate / ethanol / 0.33 h / 0 °C

6: toluene-4-sulfonic acid / dichloromethane / 20 °C / Inert atmosphere

7: diisobutylaluminium hydride / tetrahydrofuran / 3.5 h / -30 - 0 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; N-chloro-succinimide; sodium methylate; silica gel; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;