N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

Base Information

Chemical Name:N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine
CAS No.:182319-86-4
Molecular Formula:C₂₅H₃₃NO₇S
Molecular Weight:491.606
Hs Code.:

Synonyms:N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

Suppliers and Price of N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

Chemical Property:

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Technology Process of N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

There total 4 articles about N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 182319-85-3
N-(4-methoxybenzenesulfonyl)-O-benzyl-D-valine

: 5292-43-3
bromoacetic acid tert-butyl ester

: 182319-86-4
N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1021/jm800964f

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 182319-86-4
N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 1,4-dioxane; water / 20 °C

2: triethylamine / acetonitrile / Reflux

3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

With potassium carbonate; triethylamine; potassium iodide; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm200593b

Reference yield:

: 640-68-6,25609-85-2,7004-03-7,921-10-8
D-Val-OH

: 182319-86-4
N-(4-methoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 1,4-dioxane; water / 20 °C

2: triethylamine / acetonitrile / Reflux

3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

With potassium carbonate; triethylamine; potassium iodide; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm200593b