[(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Base Information

Chemical Name:[(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]
CAS No.:1361399-35-0
Molecular Formula:C₂₁H₄₁NO₂P₂Rh*C₃₂H₁₂BF₂₄
Molecular Weight:1367.64
Hs Code.:

[(2,6-(t-Bu<sub>2</sub>PO)2C<sub>5</sub>H<sub>3</sub>N)Rh(H<sub>2</sub>)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Synonyms:[(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

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Chemical Property of [(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

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Technology Process of [(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

There total 2 articles about [(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1361399-33-8
[(2,6-(t-Bu₂PO)2C₅H₃N)Rh(ethylene)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

: 1333-74-0
hydrogen

: 1361399-35-0
[(2,6-(t-Bu₂PO)2C₅H₃N)Rh(H₂)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Guidance literature:: In dichloromethane; byproducts: ethane; under Ar; on vac. line; soln. of Rh complex in CH2Cl2 frozen at -196°C; H2 (1 atm) admitted; warmed to ambient temp.; stirred for 8 h; volatiles removed in vac.; extd. in min. amt. of CH2Cl2; filtered through Celite; layered with pentane at -35°C;
DOI:10.1021/ic202630x