methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Base Information

Chemical Name:methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate
CAS No.:1356601-84-7
Molecular Formula:C₃₂H₂₈N₂O₅
Molecular Weight:520.585
Hs Code.:

Synonyms:methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Chemical Property of methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Technology Process of methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

There total 8 articles about methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.95%

: 4846-21-3
O-phenylhydroxylamine

: 1356601-82-5
methyl 3-cyano-3-(4-{[4-(2-oxo-2-phenylethoxy)benzyl]oxy}phenyl)propanoate

: 1356601-84-7
methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: With sodium acetate; acetic acid; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356601-84-7
methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 2 h / 20 - 80 °C

2: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 12.25 h / 0 - 20 °C

3: sodium acetate; acetic acid / 3 h / 20 °C / Inert atmosphere

With tributylphosphine; sodium acetate; potassium carbonate; acetic acid; 1,1'-azodicarbonyl-dipiperidine; In toluene; acetonitrile;

Reference yield:

: 623-05-2
(4-hydroxyphenyl)methanol

: 1356601-84-7
methyl 3-cyano-3-{4-[(4-{[(2E,2Z)-2-(phenoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 2 h / 20 - 80 °C

2: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 12.25 h / 0 - 20 °C

3: sodium acetate; acetic acid / 3 h / 20 °C / Inert atmosphere

With tributylphosphine; sodium acetate; potassium carbonate; acetic acid; 1,1'-azodicarbonyl-dipiperidine; In toluene; acetonitrile;