Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

Base Information

Chemical Name:Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride
CAS No.:100945-23-1
Molecular Formula:C₁₈H₁₈N₂O₆Se*ClH
Molecular Weight:473.772
Hs Code.:

Synonyms:Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

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Chemical Property of Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

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Technology Process of Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

There total 10 articles about Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100945-22-0
N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

: 100945-23-1
Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; 1,3-Dimethoxybenzene; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 57929-25-6
3,4-(diacetyloxy)benzoyl chloride

: 100945-23-1
Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: TEA / dioxane

2: 2 N etheric HCl / dioxane / 0.25 h / 20 °C

3: 1.) KI; 2.) NaN₃ / 1.) acetone, 15 min; acetone, 6 h, room temp.

4: 83 percent / H₂ / Pd/C (5percent Pd) / dioxane / 18 h / 2206.5 Torr

5: 97 percent / acetic acid, sodium-cyano trihydroborate / tetrahydrofuran / 4 h / 25 °C

6: 78 percent / tributyl phosphine / tetrahydrofuran / 3 h

7: 94 percent / 1,3-dimethoxy benzene, HCl-gas / dioxane / 1 h / Ambient temperature

With hydrogenchloride; sodium azide; tributylphosphine; TEA; hydrogen; sodium cyanoborohydride; acetic acid; potassium iodide; 1,3-Dimethoxybenzene; 5%-palladium/activated carbon; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 99-50-3
3,4-Dihydroxybenzoic acid

: 100945-23-1
Acetic acid 2-acetoxy-5-[2-amino-1-(4-nitro-phenylselanyl)-ethyl]-phenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 9 steps

1: 84 percent / 2 h / Heating

2: 82 percent / SOCl₂, pyridine / 1.5 h / Heating

3: TEA / dioxane

4: 2 N etheric HCl / dioxane / 0.25 h / 20 °C

5: 1.) KI; 2.) NaN₃ / 1.) acetone, 15 min; acetone, 6 h, room temp.

6: 83 percent / H₂ / Pd/C (5percent Pd) / dioxane / 18 h / 2206.5 Torr

7: 97 percent / acetic acid, sodium-cyano trihydroborate / tetrahydrofuran / 4 h / 25 °C

8: 78 percent / tributyl phosphine / tetrahydrofuran / 3 h

9: 94 percent / 1,3-dimethoxy benzene, HCl-gas / dioxane / 1 h / Ambient temperature

With pyridine; hydrogenchloride; thionyl chloride; sodium azide; tributylphosphine; TEA; hydrogen; sodium cyanoborohydride; acetic acid; potassium iodide; 1,3-Dimethoxybenzene; 5%-palladium/activated carbon; In tetrahydrofuran; 1,4-dioxane;