N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

Base Information

Chemical Name:N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin
CAS No.:100945-22-0
Molecular Formula:C₂₃H₂₆N₂O₈Se
Molecular Weight:537.428
Hs Code.:

Synonyms:N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

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Chemical Property of N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

Chemical Property:

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Technology Process of N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

There total 8 articles about N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 19188-18-2
p-nitrophenyl selenocyanate

: 93862-75-0
2-(tert-Butyloxycarbonylamino)-1-(3,4-diacetoxyphenyl)ethanol

: 100945-22-0
N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

Guidance literature:: With tributylphosphine; In tetrahydrofuran; for 3h;

Reference yield:

: 57929-25-6
3,4-(diacetyloxy)benzoyl chloride

: 100945-22-0
N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

Guidance literature:: Multi-step reaction with 6 steps

1: TEA / dioxane

2: 2 N etheric HCl / dioxane / 0.25 h / 20 °C

3: 1.) KI; 2.) NaN₃ / 1.) acetone, 15 min; acetone, 6 h, room temp.

4: 83 percent / H₂ / Pd/C (5percent Pd) / dioxane / 18 h / 2206.5 Torr

5: 97 percent / acetic acid, sodium-cyano trihydroborate / tetrahydrofuran / 4 h / 25 °C

6: 78 percent / tributyl phosphine / tetrahydrofuran / 3 h

With hydrogenchloride; sodium azide; tributylphosphine; TEA; hydrogen; sodium cyanoborohydride; acetic acid; potassium iodide; 5%-palladium/activated carbon; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 99-50-3
3,4-Dihydroxybenzoic acid

: 100945-22-0
N-(tert-Butyloxycarbonyl)-2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethanamin

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / 2 h / Heating

2: 82 percent / SOCl₂, pyridine / 1.5 h / Heating

3: TEA / dioxane

4: 2 N etheric HCl / dioxane / 0.25 h / 20 °C

5: 1.) KI; 2.) NaN₃ / 1.) acetone, 15 min; acetone, 6 h, room temp.

6: 83 percent / H₂ / Pd/C (5percent Pd) / dioxane / 18 h / 2206.5 Torr

7: 97 percent / acetic acid, sodium-cyano trihydroborate / tetrahydrofuran / 4 h / 25 °C

8: 78 percent / tributyl phosphine / tetrahydrofuran / 3 h

With pyridine; hydrogenchloride; thionyl chloride; sodium azide; tributylphosphine; TEA; hydrogen; sodium cyanoborohydride; acetic acid; potassium iodide; 5%-palladium/activated carbon; In tetrahydrofuran; 1,4-dioxane;