Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Base Information

Chemical Name:Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine
CAS No.:900791-15-3
Molecular Formula:C₃₁H₃₃F₃IN
Molecular Weight:603.509
Hs Code.:

Synonyms:Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

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Chemical Property of Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

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Technology Process of Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

There total 3 articles about Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 900791-11-9
{3-[(E)-2-(4-Dibutylamino-phenyl)-vinyl]-5-iodo-benzyl}-phosphonic acid diethyl ester

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 900791-15-3
Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.tetlet.2006.04.126

Reference yield:

: 90134-10-4
4-(N,N-dibutylamino)benzaldehyde

: 900791-15-3
Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / t-BuOK / tetrahydrofuran / 0 °C

2: 100 percent / t-BuOK / tetrahydrofuran / 0 °C

With potassium tert-butylate; In tetrahydrofuran; 1: Horner-Wadsworth-Emmons reaction / 2: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2006.04.126

Reference yield:

: 496043-74-4
tetraethyl((5-iodo-1,3-phenylene)bis(methylene))bis(phosphonate)

: 900791-15-3
Dibutyl-[4-((E)-2-{3-iodo-5-[(E)-2-(4-trifluoromethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / t-BuOK / tetrahydrofuran / 0 °C

2: 100 percent / t-BuOK / tetrahydrofuran / 0 °C

With potassium tert-butylate; In tetrahydrofuran; 1: Horner-Wadsworth-Emmons reaction / 2: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2006.04.126