3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride

Base Information

• Chemical Name: 3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride
• CAS No.: 1416171-24-8
• Molecular Formula: C₁₆H₂₁N₂O₂*Cl
• Molecular Weight: 308.808

Synonyms:3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride

Chemical Property of 3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride

Chemical Property:

Purity/Quality:

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Technology Process of 3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride

There total 2 articles about 3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-methyl-1H-imidazole (616-47-7) + 3-(chloromethyl)-5-(tert-butyl)-2-hydroxybenzaldehyde → 3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride (1416171-24-8)

Guidance literature:

In acetonitrile; at 20 ℃;

DOI:10.1021/jacs.9b04902 DOI:10.1021/jacs.9b10389

Reference yield:

2-hydroxy-5-t-butylbenzaldehyde (2725-53-3) → 3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride (1416171-24-8)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; sulfuric acid / 20 h / 70 °C / Inert atmosphere

2: acetonitrile / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; sulfuric acid; In acetonitrile;

DOI:10.1021/om3008629

Reference yield: 100.0%

3-(5-(tert-butyl)-3-formyl-2-hydroxybenzyl)-1-methyl-1H-imidazol-3-ium chloride (1416171-24-8) + (Ra)-6,6'-dimethyl-1,1'-biphenyl-2,2'-diamine (3685-05-0,3685-06-1,20261-65-8,86560-87-4) → (R)-(-)-N,N′-bis(5-tert-butyl-3-((1-methyl-1H-imidazol-3-ium)-3-ylmethyl)salicylidene)-2,2'-diamino-6,6'-dimethyl-[1,1'-biphenyl] dichloride

Guidance literature:

In ethanol; at 20 ℃; for 20h; Inert atmosphere; Molecular sieve;

DOI:10.1021/om3008629

upstream raw materials:

2-hydroxy-5-t-butylbenzaldehyde

1-methyl-1H-imidazole

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