C₉H₇BrCl₂

Base Information

• Chemical Name: C₉H₇BrCl₂
• CAS No.: 129140-95-0
• Molecular Formula: C₉H₇BrCl₂
• Molecular Weight: 265.965
• Mol file: 129140-95-0.mol

Synonyms:C₉H₇BrCl₂

Chemical Property of C₉H₇BrCl₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₉H₇BrCl₂

There total 1 articles about C₉H₇BrCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinyl magnesium bromide (1826-67-1) + 3,4-dichlorobenzaldehyde (6287-38-3) → C9H7BrCl2 (129140-95-0)

Guidance literature:

vinyl magnesium bromide; 3,4-dichlorobenzaldehyde; Inert atmosphere; Schlenk technique;

With phosphorus tribromide; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.5b03396

Reference yield: 75.0%

C9H7BrCl2 (129140-95-0) + C9H15N3O → C18H21Cl2N3O + C18H21Cl2N3O

Guidance literature:

With C₃₉H₆₀N₄O₄; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; diisopropylamine; magnesium triflate; In acetonitrile; at -20 ℃; for 56h; stereoselective reaction;

DOI:10.1039/c9sc06342k

Reference yield:

C9H7BrCl2 (129140-95-0) + phenylmagnesium bromide (100-58-3) → (-)-(S)-1,2-dichloro-4-(1-phenylallyl)benzene

Guidance literature:

C₉H₇BrCl₂; With [(4S,5S)-1,3-bis(bis(2-methylphenyl)methyl)-4,5-diphenylimidazolidin-2-ylidene]copper(I) chloride; In dichloromethane; at -78 ℃; Inert atmosphere;

phenylmagnesium bromide; In diethyl ether; dichloromethane; at -78 ℃; for 0.5h; optical yield given as %ee; regioselective reaction; Inert atmosphere;

DOI:10.1002/anie.200904676

upstream raw materials:

vinyl magnesium bromide

3,4-dichlorobenzaldehyde

Downstream raw materials:

(R)-1,2-dichloro-4-(1-phenylallyl)benzene

C₁₅H₁₂Cl₂

(+)-(S)-3-(3,4-dichlorophenyl)-3-phenylpropan-1-ol