5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

Base Information

Chemical Name:5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone
CAS No.:154052-82-1
Molecular Formula:C₂₀H₂₇NO₂S₂
Molecular Weight:377.572
Hs Code.:

Synonyms:5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

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Chemical Property of 5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

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Technology Process of 5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

There total 3 articles about 5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 154052-79-6
5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

: 74-88-4
methyl iodide

: 154052-82-1
5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; for 18h; Ambient temperature;
DOI:10.1021/jm00028a017

Reference yield:

: 139226-70-3
5-[1-[3,5-bis(1,1-dimethylethyl)-4hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolone

: 74-88-4
methyl iodide

: 5-[1-[3,5bis(1,1-dimethylethyl)-4-hydroxyphenyl]-ethylidene]-2-(methylthio)-4(5H)-thiazolone

: 154052-82-1
5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; water;

Reference yield:

: 14035-33-7
1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone

: 154052-82-1
5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NH₄OAc / toluene / 48 h / Heating

2: 93 percent / N,N-diisopropylethylamine / ethanol / 18 h / Ambient temperature

With ammonium acetate; N-ethyl-N,N-diisopropylamine; In ethanol; toluene;
DOI:10.1021/jm00028a017