5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

Base Information

Chemical Name:5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone
CAS No.:154052-79-6
Molecular Formula:C₁₉H₂₅NO₂S₂
Molecular Weight:363.545
Hs Code.:

Synonyms:5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

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Chemical Property of 5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

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Technology Process of 5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

There total 1 articles about 5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 141-84-4
2-thioxo-4-thiazolidinone

: 14035-33-7
1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone

: 154052-79-6
5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

Guidance literature:: With ammonium acetate; In toluene; for 48h; Heating;
DOI:10.1021/jm00028a017

Reference yield: 93.0%

: 154052-79-6
5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

: 74-88-4
methyl iodide

: 154052-82-1
5-[1-[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-(methylthio)-4(5H)-thiazolone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; for 18h; Ambient temperature;
DOI:10.1021/jm00028a017

Reference yield:

: 154052-79-6
5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]ethylidene]-2-thioxo-4-thiazolidinone

: [5-[1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]-ethylidene]-4,5-dihydro-4-oxo-2-thiazolyl]cyanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / N,N-diisopropylethylamine / ethanol / 18 h / Ambient temperature

2: 88 percent / t-BuOK / ethanol / 2.5 h / Heating

With potassium tert-butylate; N-ethyl-N,N-diisopropylamine; In ethanol;
DOI:10.1021/jm00028a017